Thermal Analysis
Thermal Conductivity , Gas Vapour Sorption and XRD

Thermal Analysis Thermal Conductivity and Gas Vapour Sorption

Stainless Steel Pans (Large Volume Pans)

 

Large-volume O-ring-sealed stainless-steel sample pans contain the sample in a sealed environment throughout an experiment. The Viton O-ring allows formation of a seal which suppresses the vaporization of a solvent or contains a volatile reaction product, thereby eliminating the interfering effects of the heat of vaporization.

These pans are crimped using the universal crimper press (B013-9005) and sealing insert (B050-5340)

 

PerkinElmer Part Number Material Temperature range
     
03190218 Pack of 20 Large volume stainless steel Capsules, covers and O-rings -40 to 300°C
03190029 Pack of 1000 Large Volume Stainless Steel Capsules, Covers and O-Rings -40 to 300°C

Benefits:

Sealed capsules prevent any mass loss

Capsules can withstand an internal pressure of 24 atm

High internal pressure capability allows water samples to be heated higher than 100°C

Large sample capacity of 60ml yields higher sensitivity

Operating range of –40°C to 300°C unless otherwise limited by sample vapor pressure

Applications:

The large-volume O-ring-sealed stainless-steel sample pan is used in the study of aqueous biological solutions (such as protein in water) where the dilution requires large sample sizes and water vaporization must be suppressed. They are also used in epoxy and phenolic curing and vulcanization of rubber where the loss of volatiles can otherwise make interpretation difficult

 

 

Thermal Analysis Differential Scanning Calorimeters, Thermogravimetic Analysers, Dynamic Mechanical Analyers, Simultaneous Thermal Analyser

Thermal Conductivity Analysers HotDisk TPS2500, TPS1500, TPS500

Gas Vapour Sorption, IGASorp, IGA,HTP

Evolved Gas Analysis TGA-MS, TGA-FTIR, TGA-GC/MS, DSC Raman

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