Thermal Analysis
Thermal Conductivity , Gas Vapour Sorption and XRD

Thermal Analysis Thermal Conductivity and Gas Vapour Sorption

Volatile and Vapour Pressure Pans

 

volatilepan.gif (3070 bytes)

 

Volatile sample pans are used with volatile solid or liquid samples which exert significant vapor pressure at the temperature of interest. They are available in both aluminum and gold.

They are sealed using the Universal Crimper press (B013-9005) and sealing insert (B014-4637)

 

PerkinElmer Part Number Material Temperature range
     
0219-0062 Aluminium -170 to 600°C
N519-0788 Aluminium (50m hole) -170 to 600°C

Benefits :

They can withstand an internal pressure of 2 atm (30 psi).

Aqueous solutions can be scanned up to and through 100°C to observe solute behavior.

The heats of fusion of materials that sublime can be determined can be determined accurately.

The effect of an enclosed atmosphere on thermal behavior of a sample can be observed.

These are small sample pans with have an effective volume of 10 ml

Covers with 50m-pinhole lids are available for measurement of boiling points, heats of vaporization, and sublimation temperatures.

 

Applications:

The major applications for this type of pan are purity analyses (i.e., pharmaceuticals, melting of lipids or liquid crystals) and phase transitions, heat of vaporization, and boiling points.

 

 

Thermal Analysis Differential Scanning Calorimeters, Thermogravimetic Analysers, Dynamic Mechanical Analyers, Simultaneous Thermal Analyser

Thermal Conductivity Analysers HotDisk TPS2500, TPS1500, TPS500

Gas Vapour Sorption, IGASorp, IGA,HTP

Evolved Gas Analysis TGA-MS, TGA-FTIR, TGA-GC/MS, DSC Raman

2010 Thermal Instruments Ltd. email tim.mann@thermal-instruments.com